In my experience if a female doesn't wag her tail or scent up the tub in the first 20 minutes of introducing a male they won't be having relations during that pairing
I let them frolic in their scented up tub even if the female defecates.
I won't break up a pairing till they decide it's done, then I go in and separate them and clean the females tub and all is back to normal.
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